Phosphorus oxychloride → 3-Chloro-7-ethyl-6,7,8,9-tetrahydro-5H-pyrido[3,4-d]azepine

HRID 400109노트

반응식

HRID 400109 반응식
Cl.Cl.O[C:4]1[N:16]=[CH:15][C:7]2[CH2:8][CH2:9][N:10]([CH2:13][CH3:14])[CH2:11][CH2:12][C:6]=2[CH:5]=1.P(Cl)(Cl)([Cl:19])=O>>[Cl:19][C:4]1[N:16]=[CH:15][C:7]2[CH2:8][CH2:9][N:10]([CH2:13][CH3:14])[CH2:11][CH2:12][C:6]=2[CH:5]=1

참가 물질

3

반응물 2

HCID 24813Phosphorus oxychlorideHCID 178462500HCID 178462500, 화합물

생성물 1

HCID 189436073-Chloro-7-ethyl-6,7,8,9-tetrahydro-5H-pyrido[3,4-d]azepine

실험 절차

Prepared from 3-hydroxy-7-ethyl-6,7,8,9-tetrahydro-5H-pyrido[3,4-d]azepine dihydrochloride by reaction with phosphorus oxychloride at 130° C.

출처 및 근거

ORD 기록
ord-0e26e0f32e74465d88d1bc9bae21568f
출처 데이터셋
uspto-grants-1998_10
특허 번호
US05827849

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