Hydrogen Bromide → HCID 49758827, 화합물

HRID 40557

반응식

C[O:2][C:3]1[CH:8]=[CH:7][C:6]([C@@H:9]([NH2:11])[CH3:10])=[CH:5][CH:4]=1.[BrH:12]>>[BrH:12].[NH2:11][C@H:9]([C:6]1[CH:7]=[CH:8][C:3]([OH:2])=[CH:4][CH:5]=1)[CH3:10]

참가 물질

반응물 2

HCID 260Hydrogen Bromide

HCID 793467(S)-1-(4-Methoxyphenyl)ethylamine

생성물 1

HCID 49758827HCID 49758827, 화합물

반응 조건

온도: 100 °C

실험 절차

To 11.0 g (72.7 mmol) (S)-1-(4-methoxy-phenyl)-ethylamine is added carefully 30 mL HBr (30% in HOAc). The mixture is stirred at 100° C. for 4 h. After cooling down to r.t., the solvent is removed in vacuo and the residue is dried in vacuo. The resulting product is used without further purification.

후처리

temperatureAfter cooling down to r.t.
customthe solvent is removed in vacuo
customthe residue is dried in vacuo
customThe resulting product is used without further purification

출처 및 근거

ORD 기록: ord-388579f90eae45a381a7f25c01287e36
출처 데이터셋: uspto-grants-2013_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08530460B2

연결된 노트

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