Methylamine → n-Methyl-3-nitropyridin-4-amine
반응식
CO[C:3]1[CH:8]=[CH:7][N:6]=[CH:5][C:4]=1[N+:9]([O-:11])=[O:10].[CH3:12][NH2:13]>C(O)C>[CH3:12][NH:13][C:3]1[CH:8]=[CH:7][N:6]=[CH:5][C:4]=1[N+:9]([O-:11])=[O:10]참가 물질
4
실험 절차
2.36 g 4-methoxy-3-nitro-pyridine and 2.33 ml methylamine (40% in water) are refluxed in 25 ml of ethanol for 3 h. Then the reaction mixture is evaporated to dryness. 2.3 g product are obtained as a solid.
후처리
- customThen the reaction mixture is evaporated to dryness
출처 및 근거
- ORD 기록
- ord-35e601a38c5e47dfb5ec3c8613cdef1f
- 출처 데이터셋
- uspto-grants-2014_06
- 특허 번호
- US08754073B2
반응 노트
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