Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylamine → (4-Methanesulfonyl-2-nitro-phenyl)methyl-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylamine | HCID 6329 | — |
| 반응물 | 1-Fluoro-4-methanesulfonyl-2-nitrobenzene | HCID 313137 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | (4-Methanesulfonyl-2-nitro-phenyl)methyl-amine | HCID 44518858 | — |
반응 단계
(4-Methanesulfonyl-2-nitro-phenyl)methyl-amine (182 mg) was prepared by following General Procedure A starting from 1-fluoro-4-methanesulfonyl-2-nitro-benzene (219 mg) and methylamine (2 M in THF, 1.0 ml) in DMF (5 mL). The crude product was used in the next step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08759535B2 |
| 출처 데이터셋 | uspto-grants-2014_06 |
| ORD ID | ord-a2c85c829b5f41c3b433ff9774433725 |
| 출처 메모 | uspto-grants-2014_06 |