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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 411049생성일: 2026년 10월 25일

Thionyl Chloride → 4-(Methylamino)-3-nitrobenzoyl chloride

https://huagongshe.com/reaction/411049

반응식

참여 물질

역할이름HCID투입량
반응물Thionyl ChlorideHCID 24386—
반응물4-(Methylamino)-3-nitrobenzoic acidHCID 283475—
생성물4-(Methylamino)-3-nitrobenzoyl chlorideHCID 17946449—

반응 조건

온도80 °C

반응 단계

4-Methylamino-3-nitro-benzoyl chloride (4.3 g) was prepared starting from 4-methylamino-3-nitro-benzoic acid (4 g) in thionyl chloride (20 mL). The reaction was heated to 80° C. for 8 h. The solvent was evaporated to isolate pure compound without any further purification.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08759535B2
출처 데이터셋uspto-grants-2014_06
ORD IDord-cf67af8299fd443997516bc33d342552
출처 메모uspto-grants-2014_06