반응식
[CH3:1][NH:2][C:3]1[CH:15]=[CH:14][C:6]([C:7]([NH:9][CH2:10][C:11]([OH:13])=O)=[O:8])=[CH:5][C:4]=1[N+:16]([O-:18])=[O:17].[CH3:19][NH:20][CH3:21].CN(C(ON1N=NC2C=CC=CC1=2)=[N+](C)C)C.F[P-](F)(F)(F)(F)F.CCN(C(C)C)C(C)C>C1COCC1.CN(C=O)C>[CH3:19][N:20]([CH3:21])[C:11]([CH2:10][NH:9][C:7](=[O:8])[C:6]1[CH:14]=[CH:15][C:3]([NH:2][CH3:1])=[C:4]([N+:16]([O-:18])=[O:17])[CH:5]=1)=[O:13]참가 물질
7
반응물 4
생성물 1
시약·촉매·용매 2
실험 절차
N-Dimethylcarbamoylmethyl-4-methylamino-3-nitro-benzamide (800 mg) was prepared by following General Procedure F starting from (4-methylamino-3-nitro-benzoylamino)-acetic acid (800 mg), 2 M dimethylamine in THF (3 mL), HBTU (1.5 g), and DIEA (1.3 mL) in DMF (2 mL).
출처 및 근거
- ORD 기록
- ord-8cb6145d254c40abaa9eb02496e625d1
- 출처 데이터셋
- uspto-grants-2014_06
- 특허 번호
- US08759535B2
연결된 노트
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