Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → 1-Acetyl-7-methylindoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 7-Methyl-2,3-dihydro-1H-indole | HCID 12377788 | — |
| 생성물 | 1-Acetyl-7-methylindoline | HCID 14361366 | — |
반응 단계
A solution of 7-methylindoline (10.2 g) in acetic anhydride (25 ml) was refluxed for 30 min. After cooling, the reaction solution was poured into ice water (250 ml) and the resulting crystal was filtered by means of suction, heated and vacuum dried to yield the end product (11.7 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06559149B1 |
| 출처 데이터셋 | uspto-grants-2003_05 |
| ORD ID | ord-532146205184410b96c1b186bb23c4a5 |
| 출처 메모 | uspto-grants-2003_05 |