Phosphoric Acid → Zirconium phosphate

HRID 41228

반응식

HRID 41228 반응식
[P:1]([O-:5])([O-:4])([O-:3])=[O:2].[P:6](=[O:10])([OH:9])([OH:8])[OH:7].[Zr:11]>>[P:1]([O-:5])([O-:4])([O-:3])=[O:2].[Zr+4:11].[P:6]([O-:10])([O-:9])([O-:8])=[O:7].[P:1]([O-:5])([O-:4])([O-:3])=[O:2].[P:1]([O-:5])([O-:4])([O-:3])=[O:2].[Zr+4:11].[Zr+4:11]

참가 물질

4

반응물 3

HCID 1004Phosphoric AcidHCID 1061PhosphateHCID 23995Zirconium

생성물 1

HCID 160986Zirconium phosphate

반응 조건

온도
350 °C

실험 절차

A zirconium phosphate film was prepared by adding a stoichometric amount of phosphate in the form of phosphoric acid to a solution of zirconium bound to PEI. The solution was then spin coated onto a glass slide and thermally treated at 1° C. to 120° C. with a dwell time of 30 minutes followed by heating to 350° C. at 1° C./minute with a dwell time of 30 minutes followed by heating to 450° C. at 1° C./minute with a dwell time of 1 hour and then cooling to 25° C.

후처리

  1. additionthermally treated at 1° C. to 120° C. with a dwell time of 30 minutes
  2. temperatureby heating to 450° C. at 1° C./minute with a dwell time of 1 hour
  3. temperaturecooling to 25° C.

출처 및 근거

ORD 기록
ord-cf4b6531eeb34d11a932e26327e1f566
출처 데이터셋
uspto-grants-2013_09
특허 번호
US08530554B1

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