p-n-Octadecyloxybenzoic acid → HCID 18521013, 화합물

HRID 413634

반응식

HRID 413634 반응식
C[O:2][C:3](=[O:21])[C:4]1[CH:9]=[CH:8][C:7]([O:10][CH2:11]/[CH:12]=[CH:13]/[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])=[CH:6][CH:5]=1.O.[OH-].[Li+].C(OC1C=CC(C(O)=O)=CC=1)CCCCCCCCCCCCCCCCC>CO>[CH2:11]([O:10][C:7]1[CH:6]=[CH:5][C:4]([C:3]([OH:21])=[O:2])=[CH:9][CH:8]=1)/[CH:12]=[CH:13]/[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]

참가 물질

5

반응물 3

HCID 139993p-n-Octadecyloxybenzoic acidHCID 168937Lithium hydroxide, monohydrateHCID 18521070Methyl-4-(trans-2-decenyloxy)-benzoate

생성물 1

HCID 18521013HCID 18521013, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

The ester 35g 565 mg, 1.95 mmol), and lithium hydroxide monohydrate (817 mg, 19.5 mmol) in 20 ml methanol were reacted according to the procedure for compound 36a. The yield was 482 mg (89% of a white powder.

출처 및 근거

ORD 기록
ord-ccede109ff2a4b66956b2756cfc70ce9
출처 데이터셋
uspto-grants-2003_05
특허 번호
US06569504B1

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