alpha-Pentyl-3-(2-quinolinylmethoxy)benzenemethanol → HCID 21280496, 화합물

HRID 414844노트

반응식

HRID 414844 반응식
[OH:1][CH:2]([C:8]1[CH:9]=[C:10]([CH:23]=[CH:24][CH:25]=1)[O:11][CH2:12][C:13]1[CH:22]=[CH:21][C:20]2[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=2)[N:14]=1)[CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[C:26](OC(=O)C)(=[O:28])[CH3:27]>N1C=CC=CC=1>[C:26]([O:1][CH:2]([C:8]1[CH:9]=[C:10]([CH:23]=[CH:24][CH:25]=1)[O:11][CH2:12][C:13]1[CH:22]=[CH:21][C:20]2[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=2)[N:14]=1)[CH2:3][CH2:4][CH2:5][CH2:6][CH3:7])(=[O:28])[CH3:27]

참가 물질

4

반응물 2

HCID 5059alpha-Pentyl-3-(2-quinolinylmethoxy)benzenemethanolHCID 7918Acetic Anhydride

생성물 1

HCID 21280496HCID 21280496, 화합물

시약·촉매·용매 1

HCID 1049Pyridine용매

실험 절차

To a solution of 2-[[3-(1-hydroxyhexyl)phenoxymethyl]quinoline (1.7 g) in pyridine at 0° C. was added acetic anhydride (2.7 ml). The reaction mixture was stirred overnight at room temperature. The solvent was removed in vacuo to obtain the crude product.

후처리

  1. customThe solvent was removed in vacuo

출처 및 근거

ORD 기록
ord-50b4618c1f9f4b10b3d8c69a0b25365b
출처 데이터셋
uspto-grants-1988_12
특허 번호
US04794188

반응 노트

불러오는 중…