Triethylamine → Triethylammonium trifluoromethanesulfonate

반응식

[F:1][C:2]([F:8])([F:7])[S:3]([OH:6])(=[O:5])=[O:4].[CH2:9]([N:11]([CH2:14][CH3:15])[CH2:12][CH3:13])[CH3:10]>>[F:1][C:2]([F:8])([F:7])[S:3]([O-:6])(=[O:5])=[O:4].[CH2:9]([NH+:11]([CH2:14][CH3:15])[CH2:12][CH3:13])[CH3:10]

참가 물질

반응물 2

HCID 8471Triethylamine2회

HCID 62406Trifluoromethanesulfonic acid2회

생성물 1

HCID 14718426Triethylammonium trifluoromethanesulfonate

실험 절차

Equimolar amounts of triethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed triethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

후처리

temperaturewhile being cooled by liquid nitrogen
customthus obtaining a target ionic conductor

출처 및 근거

ORD 기록: ord-a75f31e657b84c399714d8636269916a
출처 데이터셋: uspto-grants-2013_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08535849B2

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