Sodium Hydroxide → Sodium 4-ethenylnaphthalenesulfonate

반응식

Br[CH2:2][CH2:3][C:4]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[C:7]([S:14]([OH:17])(=[O:16])=[O:15])=[CH:6][CH:5]=1.[OH-].[Na+:19]>>[CH:3]([C:4]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[C:7]([S:14]([O-:17])(=[O:15])=[O:16])=[CH:6][CH:5]=1)=[CH2:2].[Na+:19]

참가 물질

반응물 2

HCID 14798Sodium Hydroxide

HCID 866126914-(2-Bromoethyl)naphthalenesulfonic acid

생성물 1

HCID 86612692Sodium 4-ethenylnaphthalenesulfonate

실험 절차

Next, 4-(2-bromoethyl)naphthalenesulfonic acid (10 g) was slowly added dropwise to a 1-mol/L aqueous solution of sodium hydroxide (100 mL), and the whole was stirred for 1 hour at room temperature. After that, the resultant was refluxed for 6 hours, and was then subjected to a dehydrobromination reaction, whereby sodium 4-ethenylnaphthalenesulfonate was obtained.

후처리

temperatureAfter that, the resultant was refluxed for 6 hours
customwas then subjected to a dehydrobromination reaction

출처 및 근거

ORD 기록: ord-2ac93d6b7a6e4713af8aa13ce7509ead
출처 데이터셋: uspto-grants-2012_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08093342B2

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