Phenol → HCID 57942486, 화합물

HRID 418978

반응식

HRID 418978 반응식
Br[C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][C:5]([Cl:11])=[CH:4][N:3]=1.[C:12]1([OH:18])[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.C([O-])([O-])=O.[K+].[K+]>CN(C=O)C>[Cl:11][C:5]1[CH:6]=[C:7]([N+:8]([O-:10])=[O:9])[C:2]([O:18][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[N:3][CH:4]=1

참가 물질

5

반응물 3

HCID 996PhenolHCID 11430Potassium CarbonateHCID 2806812-Bromo-5-chloro-3-nitropyridine

생성물 1

HCID 57942486HCID 57942486, 화합물

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

This compound was prepared according to the general procedure A described above using 2-bromo-5-chloro-3-nitro-pyridine (500 mg, 2.11 mmol), phenol (258 mg, 2.75 mmol), K2CO3 (437 mg, 3.16 mmol) and DMF (2 mL). MS m/z: 250.4 (M+H).

후처리

  1. customThis compound was prepared

출처 및 근거

ORD 기록
ord-4fa2b5c3fa9f47c99e5f5fba3e886dab
출처 데이터셋
uspto-grants-2012_01
특허 번호
US08093247B2

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