Hydrochloric Acid → methyl 1H-tetrazol-1-ylacetate

HRID 419839노트

반응식

HRID 419839 반응식
[N:1]1([CH2:6][C:7]([OH:9])=[O:8])[CH:5]=[N:4][N:3]=[N:2]1.Cl.O1CCOC[CH2:12]1>CO>[N:1]1([CH2:6][C:7]([O:9][CH3:12])=[O:8])[CH:5]=[N:4][N:3]=[N:2]1

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 312751,4-DioxaneHCID 5432071-Tetrazolylacetic acid

생성물 1

HCID 3153776methyl 1H-tetrazol-1-ylacetate

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

A mixture of tetrazol-1-yl acetic acid (5 g, 39 mmol) and 4M hydrochloric acid in dioxan (100 μL) in methanol (50 mL) was heated under reflux for 18 hours. The cooled mixture was evaporated under reduced pressure to provide the title compound.

후처리

  1. temperaturewas heated
  2. temperatureunder reflux for 18 hours
  3. customThe cooled mixture was evaporated under reduced pressure

출처 및 근거

ORD 기록
ord-1f14cc65617e4ae1985a9137fda2cfc7
출처 데이터셋
uspto-grants-2012_01
특허 번호
US08093400B2

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