3,5-Dichloroaniline → N-(3,5-Dichlorophenyl)-2-hydroxy-1-naphthamide

HRID 421017

반응식

HRID 421017 반응식
[OH:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]=1[C:12]([OH:14])=O.[Cl:15][C:16]1[CH:17]=[C:18]([CH:20]=[C:21]([Cl:23])[CH:22]=1)[NH2:19]>>[Cl:15][C:16]1[CH:17]=[C:18]([NH:19][C:12]([C:3]2[C:4]3[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=3)[CH:10]=[CH:11][C:2]=2[OH:1])=[O:14])[CH:20]=[C:21]([Cl:23])[CH:22]=1

참가 물질

3

반응물 2

HCID 122813,5-DichloroanilineHCID 167902-Hydroxy-1-naphthoic acid

생성물 1

HCID 11724295N-(3,5-Dichlorophenyl)-2-hydroxy-1-naphthamide수율 51.2%

실험 절차

Using 2-hydroxynaphthalene-1-carboxylic acid and 3,5-dichloroaniline as the raw materials, the same operation as the example 16 gave the title compound.

출처 및 근거

ORD 기록
ord-d3a0ea052945469aab1c46aaddbaa0cd
출처 데이터셋
uspto-grants-2012_01
특허 번호
US08097759B2

연결된 노트

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