Methylene blue cation → Methylene blue neutral red

HRID 421532

반응식

HRID 421532 반응식
[CH3:1][N:2]([C:4]1[CH:5]=[CH:6][C:7]2[N:20]=[C:19]3[C:11](=[CH:12][C:13]([CH:17]=[CH:18]3)=[N+:14]([CH3:16])[CH3:15])[S:10][C:8]=2[CH:9]=1)[CH3:3].[CH3:21][C:22]1[C:38]([NH2:39])=[CH:37][C:36]2[C:24](=[N:25][C:26]3[CH:31]=[CH:30][C:29]([N:32]([CH3:34])[CH3:33])=[CH:28][C:27]=3[N:35]=2)[CH:23]=1.[ClH:40]>>[CH3:3][N:2]([C:4]1[CH:5]=[CH:6][C:7]2[N:20]=[C:19]3[C:11](=[CH:12][C:13]([CH:17]=[CH:18]3)=[N+:14]([CH3:15])[CH3:16])[S:10][C:8]=2[CH:9]=1)[CH3:1].[CH3:21][C:22]1[C:38]([NH2:39])=[CH:37][C:36]2[C:24](=[N:25][C:26]3[CH:31]=[CH:30][C:29]([N:32]([CH3:34])[CH3:33])=[CH:28][C:27]=3[N:35]=2)[CH:23]=1.[ClH:40]

참가 물질

3

반응물 2

HCID 4139Methylene blue cationHCID 11105Neutral Red

생성물 1

HCID 131729400Methylene blue neutral red

반응 조건

온도
50 °C

실험 절차

Cream-methylene blue/neutral red swatches were prepared by mixing 13.2 mg of methylene blue (Merck no. 14279) and 15.0 mg of neutral red (Merck no. 1369) with 100 g cream (38% fat, not homogenised) at 50° C., the mixture was left at this temperature for 20 minutes and filtered to remove any undissolved particles. Woven cotton swatches were immersed in the cream-methylene blue/neutral red mixture and afterwards allowed to dry at room temperature over night and frozen until use.

후처리

  1. filtrationfiltered
  2. customto remove any undissolved particles
  3. customto dry at room temperature over night
  4. temperaturefrozen until use

출처 및 근거

ORD 기록
ord-6cdc028ddd4c426c907ac35e00a98c85
출처 데이터셋
uspto-grants-2012_01
특허 번호
US08101376B2

연결된 노트

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