1,1,1-Trifluoro-2-propanol → HCID 25129833, 화합물

HRID 422552노트

반응식

HRID 422552 반응식
[F:1][C:2]([F:7])([F:6])[CH:3]([OH:5])[CH3:4].[H-].[Na+].[Br:10][C:11]1[CH:12]=[C:13]2[C:18](=[CH:19][CH:20]=1)[C:17](Cl)=[N:16][N:15]=[CH:14]2>>[Br:10][C:11]1[CH:12]=[C:13]2[C:18](=[CH:19][CH:20]=1)[C:17]([O:5][CH:3]([CH3:4])[C:2]([F:7])([F:6])[F:1])=[N:16][N:15]=[CH:14]2

참가 물질

4

반응물 3

HCID 97741,1,1-Trifluoro-2-propanolHCID 24758Sodium hydrideHCID 220304246-Bromo-1-chlorophthalazine

생성물 1

HCID 25129833HCID 25129833, 화합물

실험 절차

This compound was prepared according to the procedure described in Example 2b, but starting with 1,1,1-trifluoropropan-2-ol, sodium hydride and 6-bromo-1-chlorophthalazine. MS (ESI, pos. ion) m/z: 321.9 (M+1).

후처리

  1. customThis compound was prepared

출처 및 근거

ORD 기록
ord-598bce3eb55a41db9e44a59aef346a39
출처 데이터셋
uspto-grants-2012_01
특허 번호
US08101612B2

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