Benzoyl chloride → 1-Phenyl-2-(4-pyridyl)vinyl benzoate

HRID 42555노트

반응식

[C:1]1([C:7](=[O:15])[CH2:8][C:9]2[CH:14]=[CH:13][N:12]=[CH:11][CH:10]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:16](Cl)(=[O:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[C:16]([O:15][C:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)=[CH:8][C:9]1[CH:10]=[CH:11][N:12]=[CH:13][CH:14]=1)(=[O:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

참가 물질

반응물 2

HCID 7412Benzoyl chloride

HCID 2871041-Phenyl-2-(4-pyridinyl)ethanone

생성물 1

HCID 684443451-Phenyl-2-(4-pyridyl)vinyl benzoate수율 62%

실험 절차

Following a similar procedure to that described in reference example 4, but using 1-phenyl-2-(4-pyridyl)ethanone (obtained in reference example 3) instead of 1-(4-fluorophenyl)-2-(4-pyridyl)ethanone and benzoyl chloride instead of 4-fluorobenzoyl chloride, the title compound was obtained (yield: 62%).

출처 및 근거

ORD 기록: ord-8d665b0c425a4fc6af6eba343ee489ec
출처 데이터셋: uspto-grants-2013_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08536194B2

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