Cyclohexanone → Cyclohexylbenzene

HRID 426466

반응식

HRID 426466 반응식
[CH:1]1([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C1(=O)CCCCC1.C1(O)C=CC=CC=1.[O-]O.C1(C2C=CC=CC=2)CCCCC1.C1(=O)CCCCC1>>[CH:7]1([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12]1

참가 물질

4

반응물 3

HCID 7967CyclohexanoneHCID 70592972Cyclohexylbenzene cyclohexanone phenolHCID 86589629Cyclohexylbenzene hydroperoxide

생성물 1

HCID 13229Cyclohexylbenzene

실험 절차

A cyclohexylbenzene-cyclohexanone-phenol-containing mixture, for example as obtained by the cleavage of cyclohexylbenzene hydroperoxide, is separated by first catalytically hydrogenating selectively the phenol in the mixture, resulting in a mixture of cyclohexylbenzene, which is unchanged, and cyclohexanone; the thus obtained mixture is subjected to fractional distillation to obtain cyclohexylbenzene which can be returned as to a process for the production of cyclohexylbenzene hydroperoxide, and cyclohexanone.

후처리

  1. customis separated by first catalytically hydrogenating selectively the phenol in the mixture
  2. customresulting in a mixture of cyclohexylbenzene, which
  3. distillationthe thus obtained mixture is subjected to fractional distillation

출처 및 근거

ORD 기록
ord-26eda82f98e140b6ae5d33a96f7e8bdf
출처 데이터셋
uspto-grants-1979_10
특허 번호
US04169857

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