Cyclohexanone → Cyclohexanone

HRID 426586

반응식

HRID 426586 반응식
[C:1]1(=[O:7])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1>O>[C:1]1(=[O:7])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[C:1]1(=[C:2]2[CH2:3][CH2:4][CH2:5][CH2:6][C:1]2=[O:7])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

참가 물질

4

반응물 1

HCID 7967Cyclohexanone

생성물 2

HCID 7967CyclohexanoneHCID 13892Bicyclohexyliden-2-one

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Using the equipment from Example 15, 1500 ml cyclohexanone was charged to the flask with 100 g aluminum oxycarbonate. The flask was heated to an initial boiling point of 142 degrees C. Water evolved quickly and the temperature rose to 200 degrees C. in three hours. The fluid was decanted and distilled yielding unreacted cyclohexanone along with cyclohexylidene cyclohexanone and the higher condensation product C18H26O believed to be dicyclohexylidene cyclohexanone.

후처리

  1. temperatureThe flask was heated to an initial boiling point of 142 degrees C
  2. customrose to 200 degrees C
  3. customThe fluid was decanted
  4. distillationdistilled

출처 및 근거

ORD 기록
ord-91875b6c0c984e0fb4f672eb1530f989
출처 데이터셋
uspto-grants-1979_10
특허 번호
US04170609

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