Methyl iodide → HCID 178504016, 화합물

HRID 426739노트

반응식

[CH3:1][N:2]1[C:6]([NH:7][C:8]([NH2:10])=[S:9])=[CH:5][C:4]([CH3:11])=[N:3]1.[CH3:12][I:13]>>[IH:13].[CH3:1][N:2]1[C:6]([NH:7][C:8](=[NH:10])[S:9][CH3:12])=[CH:5][C:4]([CH3:11])=[N:3]1

참가 물질

반응물 2

HCID 6328Methyl iodide

HCID 12763851HCID 12763851, 화합물

생성물 1

HCID 178504016HCID 178504016, 화합물

실험 절차

(1,3-Dimethyl-5-pyrazolyl) thiourea (17.0 g) and 14.2 g methyl iodide were reacted as described in Example V to give 18.0 g. of the product, mp 158°-161° C.

후처리

customto give 18.0 g

출처 및 근거

ORD 기록: ord-e823181c95ca4f4fad09f730e75a3fad
출처 데이터셋: uspto-grants-1979_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04171367

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