O-Methylhydroxylamine → cyclohexenyl-ethanone O-methyl-oxime

HRID 42725

반응식

HRID 42725 반응식
[C:1]1([C:7](=O)[CH3:8])[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1.[CH3:10][O:11][NH2:12]>C(O)(=O)C>[CH3:10][O:11][N:12]=[C:7]([C:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1)[CH3:8]

참가 물질

4

반응 조건

온도
24 °C

실험 절차

To a stirred solution of a cyclohexenyl-ethanone (0.06 mmol), in acetic acid (500 μl) was added methoxyamine (4.7 mg). The reaction mixture was stirred at 24° C. for 48 h under nitrogen to obtain the cyclohexenyl-ethanone O-methyl-oxime.

출처 및 근거

ORD 기록
ord-57036d9ef90e40e0a656d26d4659e650
출처 데이터셋
uspto-grants-2013_09
특허 번호
US08536215B2

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