Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6-Fluoroindole → 3-(1,4-Dioxa-spiro[4,5]dec-7-en-8-yl)-6-fluoro-1H-indole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6-Fluoroindole | HCID 351278 | — |
| 반응물 | 3-(1,4-Dioxaspiro[4.5]dec-7-en-8-yl)-1H-indole | HCID 2763857 | — |
| 생성물 | 3-(1,4-Dioxa-spiro[4,5]dec-7-en-8-yl)-6-fluoro-1H-indole | HCID 18414166 | 96.3% |
반응 단계
This compound was prepared in the manner described for intermediate 1a by replacing indole with 6-fluoroindole (5.14 g, 38 mmol) ) to afford 10 g (96.3%) of the title compound as a white solid: mp 196-197° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06313126B1 |
| 출처 데이터셋 | uspto-grants-2001_11 |
| ORD ID | ord-073920222edc4c1988928536db1edb8e |
| 출처 메모 | uspto-grants-2001_11 |