Sulfuric Acid → HCID 18355456, 화합물

HRID 429338노트

반응식

HRID 429338 반응식
[I:1][C:2]1[CH:3]=[C:4]([CH:21]=[C:22]([I:25])[C:23]=1[OH:24])[C:5]([C:7]1[C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=2[O:9][C:8]=1[CH2:16][CH2:17][C:18]([OH:20])=[O:19])=[O:6].S(=O)(=O)(O)O>CC(O)CC>[I:25][C:22]1[CH:21]=[C:4]([CH:3]=[C:2]([I:1])[C:23]=1[OH:24])[C:5]([C:7]1[C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=2[O:9][C:8]=1[CH2:16][CH2:17][C:18]([O:20][CH:2]([CH2:23][CH3:22])[CH3:3])=[O:19])=[O:6]

참가 물질

4

반응물 2

HCID 1118Sulfuric AcidHCID 18355455HCID 18355455, 화합물

생성물 1

HCID 18355456HCID 18355456, 화합물

시약·촉매·용매 1

HCID 6568(+-)-2-Butanol용매

실험 절차

562 g of compound 6 are stirred at 85° C. in 900 g of 2-butanol and 50 ml of sulfuric acid for 5 hours. Cool down to room temperature. Filter the product. Wash twice with 100 ml of hexane.

후처리

  1. filtrationFilter the product
  2. washWash twice with 100 ml of hexane

출처 및 근거

ORD 기록
ord-87124c601c74420697bc1fa235218325
출처 데이터셋
uspto-grants-2001_11
특허 번호
US06316487B1

반응 노트

불러오는 중…