Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetyl chloride → Benzeneethanol, alpha-methyl-, 1-acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | 1-Phenyl-2-propanol | HCID 94185 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | Benzeneethanol, alpha-methyl-, 1-acetate | HCID 16457 | — |
반응 단계
Acetyl chloride (16.7 g) in dry ether (50 ml) was added dropwise to a stirred solution of 1-phenylpropan-2-ol (26.4 g) in dry ether (250 ml). The mixture was refluxed for 2 h, washed with sodium bicarbonate solution, dried (MgSO4) and evaporated to a colourless oil (27.5 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04396627 |
| 출처 데이터셋 | uspto-grants-1983_08 |
| ORD ID | ord-503077e2db97420c8662fa1b6b958cd4 |
| 출처 메모 | uspto-grants-1983_08 |