反应详情

Acetyl chloride (16.7 g) in dry ether (50 ml) was added dropwise to a stirred solution of 1-phenylpropan-2-ol (26.4 g) in dry ether (250 ml). The mixture was refluxed for 2 h, washed with sodium bicarbonate solution, dried (MgSO4) and evaporated to a colourless oil (27.5 g).

1. temperatureThe mixture was refluxed for 2 h
2. washwashed with sodium bicarbonate solution
3. dry with materialdried (MgSO4)
4. customevaporated to a colourless oil (27.5 g)