Sodium Hydroxide → 1-(4-Acetylphenyl) propan-2-ol

반응식

C([O:4][CH:5]([CH3:16])[CH2:6][C:7]1[CH:12]=[CH:11][C:10]([C:13](=[O:15])[CH3:14])=[CH:9][CH:8]=1)(=O)C.[OH-].[Na+]>>[C:13]([C:10]1[CH:11]=[CH:12][C:7]([CH2:6][CH:5]([OH:4])[CH3:16])=[CH:8][CH:9]=1)(=[O:15])[CH3:14]

참가 물질

반응물 2

HCID 14798Sodium Hydroxide

HCID 204938272-Acetoxy-1-(4-acetylphenyl)propane

생성물 1

HCID 225984461-(4-Acetylphenyl) propan-2-ol수율 104.4%

실험 절차

2-Acetoxy-1-(4-acetylphenyl) propane (4.5 g) was heated for 2 hours in refluxing 2 N sodium hydroxide solution. The mixture was allowed to cool and the product was extracted into ether. Evaporation of the dried (MgSO4) extracts gave an oil (3.8 g).

후처리

temperatureto cool
extractionthe product was extracted into ether
customEvaporation of the
dry with materialdried (MgSO4)

출처 및 근거

ORD 기록: ord-f3d02f20e0444b7eb09a5c9a270b63d0
출처 데이터셋: uspto-grants-1983_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04396627

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