Sodium → D-glycero-D-gulo-heptonic acid

HRID 434492

반응식

HRID 434492 반응식
[Na].[CH2:2]([OH:16])[C@@H:3]([OH:15])[C@@H:4]([OH:14])[C@H:5]([OH:13])[C@@H:6]([OH:12])[C@@H:7]([OH:11])[C:8]([O-:10])=[O:9].[Na+]>O.O[Mo](O)(=O)=O>[CH2:2]([OH:16])[C@@H:3]([OH:15])[C@@H:4]([OH:14])[C@H:5]([OH:13])[C@@H:6]([OH:12])[C@@H:7]([OH:11])[C:8]([OH:10])=[O:9]

참가 물질

5

반응물 2

HCID 5360545SodiumHCID 23664054Gluceptate Sodium

생성물 1

HCID 25588D-glycero-D-gulo-heptonic acid

시약·촉매·용매 2

HCID 82208Molybdic acid촉매HCID 962Water용매2회

반응 조건

온도
25 °C

실험 절차

The molybdenum ester of glucoheptonic acid was prepared as follows: Approximately 241 grams (1 mol) of the sodium salt of molybdic acid (sodium molybdenate) and 248 grams (1 mol) of sodium glucoheptonate were charged to an esterification vessel containing about 600 ml. of water as a solvent. With stirring, the temperature was maintained at about 25° C. for approximately 30 minutes. The mixture was thereafter diluted to a final volume of one liter with additional water.

후처리

  1. additioncontaining about 600 ml

출처 및 근거

ORD 기록
ord-7d201175ba1b4101920c7c473c66295e
출처 데이터셋
uspto-grants-1983_08
특허 번호
US04397812

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