Sodium Carbonate → N-Hydroxy-5-norbornene-2,3-dicarboxylic acid imide

HRID 434758

반응식

HRID 434758 반응식
[CH:1]12[CH2:7][CH:4]([CH:5]=[CH:6]1)[CH:3]1[C:8]([O:10][C:11](=[O:12])[CH:2]21)=[O:9].C(=O)([O-])[O-].[Na+].[Na+].Cl.[NH2:20][OH:21]>O>[OH:21][N:20]=[C:11]([CH:2]1[CH:3]([C:8]([OH:10])=[O:9])[CH:4]2[CH2:7][CH:1]1[CH:6]=[CH:5]2)[OH:12]

참가 물질

5

반응물 3

HCID 10340Sodium CarbonateHCID 13223826-62-0HCID 443297Hydroxyamine hydrochloride

생성물 1

HCID 178524005N-Hydroxy-5-norbornene-2,3-dicarboxylic acid imide

시약·촉매·용매 1

HCID 962Water용매

실험 절차

30 ml of water was added to 24.6 g of 5-norbornene-2,3-dicarboxylic acid anhydride, and while cooling the reaction temperature below 20° C., 10.6 g of sodium carbonate and then 13.9 g of hydroxylamine hydrochloride were added. The mixture was reacted at room temperature for 1 hour and then reacted at a temperature of 60° to 70° C. for 1 hour. After cooling to room temperature, N-hydroxy-5-norbornene-2,3-dicarboxylic acid imide thus formed was collected by filtration.

후처리

  1. customThe mixture was reacted at room temperature for 1 hour
  2. customreacted at a temperature of 60° to 70° C. for 1 hour

출처 및 근거

ORD 기록
ord-6b46f60f07d04d8f8b24b76804aa1cb2
출처 데이터셋
uspto-grants-1983_08
특허 번호
US04399210

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