Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → 1-Methyl-s-triazolo[4,3-a]quinoxaline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | 2-Hydrazinoquinoxaline | HCID 289847 | — |
| 생성물 | 1-Methyl-s-triazolo[4,3-a]quinoxaline | HCID 21817404 | — |
반응 단계
A 5 g. portion of 2-hydrazinoquinoxaline was stirred at reflux temperature in acetic acid for 3 hours. The reaction mixture was then cooled, and was evaporated to dryness under vacuum. The product was found to melt at 210°-12° C. without purification, and was identified as 1-methyl-s-triazolo[ 4,3-a]quinoxaline by NMR analysis and elemental microanalysis, the results of which follow.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04008322 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-4a363311389b443a82fd6b09271767e6 |
| 출처 메모 | uspto-grants-1977_02 |