8-(2,5-Dimethoxy-tetrahydro-2-furyl)-octanoic acid methyl ester → 9-Keto-12-oxo-dodecanoic acid, methyl ester

HRID 436525노트

반응식

HRID 436525 반응식
[CH3:1][O:2][C:3](=[O:20])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][C:11]1(OC)[CH2:15][CH2:14][CH:13]([O:16]C)[O:12]1>Cl>[CH3:1][O:2][C:3](=[O:20])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][C:11](=[O:12])[CH2:15][CH2:14][CH:13]=[O:16]

참가 물질

3

반응물 1

HCID 541867608-(2,5-Dimethoxy-tetrahydro-2-furyl)-octanoic acid methyl ester

생성물 1

HCID 150938019-Keto-12-oxo-dodecanoic acid, methyl ester

시약·촉매·용매 1

HCID 313Hydrochloric Acid용매

실험 절차

10.0 g of the compound of step B was stirred for 30 minutes with 2100 ml of 1N hydrochloric acid at room temperature. The mixture was then extracted rapidly several times with ether.

후처리

  1. extractionThe mixture was then extracted rapidly several times with ether

출처 및 근거

ORD 기록
ord-24b6c66e261f407fa89e024bb3d022c9
출처 데이터셋
uspto-grants-1977_02
특허 번호
US04009187

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