2-Naphthalenecarboxaldehyde → 2-Naphthalenecarbonitrile

HRID 436673

반응식

HRID 436673 반응식
[CH:1]([C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=1)=O.Cl.[NH2:14]O.C([O-])(=O)C.[Na+]>C(O)C>[C:1]([C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=1)#[N:14]

참가 물질

5

반응물 3

HCID 62012-NaphthalenecarboxaldehydeHCID 443297Hydroxyamine hydrochlorideHCID 517045Sodium Acetate

생성물 1

HCID 119442-Naphthalenecarbonitrile

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

2-Cyanonaphthalene is prepared by refluxing 2-formylnaphthalene with hydroxylamine hydrochloride and sodium acetate in ethanol to furnish the corresponding oxime which is refluxed with acetic anhydride in the presence of an acid catalyst to furnish 2-cyanonaphthalene.

출처 및 근거

ORD 기록
ord-2a494bae047b47c2a834747d05d7d1e7
출처 데이터셋
uspto-grants-1977_02
특허 번호
US04009197

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