N,N-Dimethylallylamine → Allyl n-butoxymethyl dimethylammonium chloride

HRID 437030

반응식

HRID 437030 반응식
[CH2:1]([O:5][CH2:6][Cl:7])[CH2:2][CH2:3][CH3:4].[CH2:8]([N:11]([CH3:13])[CH3:12])[CH:9]=[CH2:10]>C(OCC)(=O)C>[Cl-:7].[CH2:8]([N+:11]([CH2:6][O:5][CH2:1][CH2:2][CH2:3][CH3:4])([CH3:13])[CH3:12])[CH:9]=[CH2:10]

참가 물질

4

반응물 2

HCID 75082N,N-DimethylallylamineHCID 111053571-(Chloromethoxy)butane

생성물 1

HCID 21429949Allyl n-butoxymethyl dimethylammonium chloride

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

24.7 grams of chloromethyl butyl ether was added to 17 grams of allyl dimethylamine in 32 grams of ethyl acetate. The reaction was highly exothermic and two layers formed very rapidly. Stirring was continued at 25° C. for 24 hours, after which the solvent was removed by vacuum. Chloride analysis of the rather viscous liquid product indicated 91% of theoretical.

후처리

  1. customtwo layers formed very rapidly
  2. customafter which the solvent was removed by vacuum

출처 및 근거

ORD 기록
ord-555e2f750b504c65a2b53b679bcae8c9
출처 데이터셋
uspto-grants-1977_06
특허 번호
US04029658

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