Lauric Acid → Silver laurate

HRID 437306

반응식

HRID 437306 반응식
[OH-].[Na+].[C:3]([OH:16])(=[O:15])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[N+]([O-])([O-])=O.[Ag+:21]>O.C1(C)C=CC=CC=1>[C:3]([O-:16])(=[O:15])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[Ag+:21]

참가 물질

6

반응물 3

HCID 3893Lauric AcidHCID 14798Sodium HydroxideHCID 24470Silver Nitrate

생성물 1

HCID 9904644Silver laurate

시약·촉매·용매 2

HCID 962Water용매2회HCID 1140Toluene용매

실험 절차

1.9 g of sodium hydroxide was dissolved in 100 ml of water, with which 12 g of lauric acid in 100 ml of toluene was mixed to emulsify (at 25° C). An aqueous solution of 8.5 g of silver nitrate dissolved in 50 ml of water was, then, added to the above emulsion to result in a separation into a silver laurate-containing toluene phase and an aqueous phase. After removal of the aqueous phase, the toluene phase was dispersed into 200 ml of ethanol, and then, silver laurate was collected by centrifuging. 12 g of spindle-like silver laurate crystals of a longer diameter of about 3 μ was obtained.

후처리

  1. additionwas mixed
  2. custom(at 25° C)
  3. additionadded to the above emulsion

출처 및 근거

ORD 기록
ord-d6b89e35ccf54dd48e695c5a31b1be27
출처 데이터셋
uspto-grants-1977_06
특허 번호
US04030931

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