Hydrochloric Acid → HCID 178501833, 화합물

HRID 440316노트

반응식

HRID 440316 반응식
[ClH:1].[NH2:2][C@H:3]1[CH2:8][CH2:7][C@H:6]([O:9][CH2:10][C:11]([O:13][C:14](C)(C)C)=[O:12])[CH2:5][CH2:4]1>CO>[ClH:1].[NH2:2][C@H:3]1[CH2:8][CH2:7][C@H:6]([O:9][CH2:10][C:11]([O:13][CH3:14])=[O:12])[CH2:5][CH2:4]1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 178451370HCID 178451370, 화합물

생성물 1

HCID 178501833HCID 178501833, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Hydrochloric acid gas is piped for an hour over a solution of 59.4 g of tert.butyl (trans-4-aminocyclohexyl)oxyacetate in 500 ml of methanol, cooled in an ice bath, and then the mixture is stirred overnight at ambient temperature. It is evaporated to dryness, the residue is triturated with acetone and the solid is suction filtered and dried.

후처리

  1. temperaturecooled in an ice bath
  2. customIt is evaporated to dryness
  3. customthe residue is triturated with acetone
  4. filtrationfiltered
  5. customdried

출처 및 근거

ORD 기록
ord-03fe03ea10134538a521ae7fd0c90598
출처 데이터셋
uspto-grants-1996_05
특허 번호
US05519036

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