Hydrochloric Acid → HCID 21193372, 화합물

HRID 443227노트

반응식

HRID 443227 반응식
[C:1]([C:3]1[CH:17]=[CH:16][C:6]([CH2:7][N:8]2[C:12]([N+:13]([O-])=O)=[CH:11][N:10]=[CH:9]2)=[CH:5][CH:4]=1)#[N:2].[ClH:18]>[Pd]>[ClH:18].[C:1]([C:3]1[CH:4]=[CH:5][C:6]([CH2:7][N:8]2[C:12]([NH2:13])=[CH:11][N:10]=[CH:9]2)=[CH:16][CH:17]=1)#[N:2]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 53889261HCID 53889261, 화합물

생성물 1

HCID 21193372HCID 21193372, 화합물

시약·촉매·용매 1

HCID 23938Palladium촉매

실험 절차

A solution of 1-(4 cyanobenzyl)-5-nitro-1H-imidazole (100 mg, 0.438 mmol) and 10% palladium on carbon was hydrogenated in the presence of 1 equivalent of HCl under Parr conditions for 1 hr. Removal of the catalyst by filtration and evaporation of solvent in vacuo afforded the title compound.

후처리

  1. customRemoval of the catalyst
  2. filtrationby filtration and evaporation of solvent in vacuo

출처 및 근거

ORD 기록
ord-0134fdf3cb2043ae937478308bd86215
출처 데이터셋
uspto-grants-1999_04
특허 번호
US05891889

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