Benzene → HCID 23464491, 화합물
반응식
O[CH2:2][C:3]1[CH:18]=[CH:17][C:6]2[C:7](=[O:16])[NH:8][C:9]3[CH:15]=[CH:14][CH:13]=[CH:12][C:10]=3[S:11][C:5]=2[CH:4]=1.C1C=CC=CC=1.P(Br)(Br)[Br:26].O>C1(C)C=CC=CC=1>[Br:26][CH2:2][C:3]1[CH:18]=[CH:17][C:6]2[C:7](=[O:16])[NH:8][C:9]3[CH:15]=[CH:14][CH:13]=[CH:12][C:10]=3[S:11][C:5]=2[CH:4]=1참가 물질
6
실험 절차
Dissolve 4.43 gm. of the alcohol of Step A in 100 cc. of benzene and add 1 cc (10.5 mmole) of phosphorous tribromide. Stir at room temperature for 1 hour, add water and then dilute with toluene. Wash three times with water, dry and strip to a solid residue.
후처리
- dissolutionDissolve 4.43 gm
- washWash three times with water
- customdry
출처 및 근거
- ORD 기록
- ord-6b4c7ac2cd9d459686713386e7887db3
- 출처 데이터셋
- uspto-grants-1981_04
- 특허 번호
- US04263207
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