Acetone → HCID 178479714, 화합물
반응식
[N:1]1([CH2:6][CH2:7][S:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2O)[CH2:5][CH2:4][CH2:3][CH2:2]1.[C:16]1([N:22]=[C:23]([Cl:30])[C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1.CC(C)=[O:33]>>[ClH:30].[N:1]1([CH2:6][CH2:7][S:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[C:25]2[CH:26]=[CH:27][CH:28]=[CH:29][C:24]=2[C:23](=[N:22][C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[OH:33])[CH2:5][CH2:4][CH2:3][CH2:2]1참가 물질
4
실험 절차
A solution of 5.5 gms (0.025 mole) of 2-[β-(1-pyrrolidinyl)ethylthio]phenol and 5.3 gms (0.025 mole) of N-phenylbenzimidoyl chloride in 50 ml acetone was stirred at room temperature for a period of two hours. The desired product crystallized out. It was filtered, washed with acetone and dried at room temperature. Recrystallization from isopropanol yielded 6.0 gms (55%) of product, M.P. 167°-9° C.
후처리
- customThe desired product crystallized out