4,4'-Dimethoxydiphenylamine → HCID 22263989, 화합물

HRID 445178

반응식

HRID 445178 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([NH:9][C:10]2[CH:15]=[CH:14][C:13]([O:16][CH3:17])=[CH:12][CH:11]=2)=[CH:5][CH:4]=1.[O-:18][C:19]#[N:20].[Na+].[OH-].[Na+]>C(O)(=O)C.O>[CH3:17][O:16][C:13]1[CH:14]=[CH:15][C:10]([N:9]([C:6]2[CH:5]=[CH:4][C:3]([O:2][CH3:1])=[CH:8][CH:7]=2)[C:19]([NH2:20])=[O:18])=[CH:11][CH:12]=1

참가 물질

6

반응물 3

HCID 75714,4'-DimethoxydiphenylamineHCID 14798Sodium HydroxideHCID 517096Sodium Cyanate

생성물 1

HCID 22263989HCID 22263989, 화합물

시약·촉매·용매 2

HCID 176Acetic Acid용매HCID 962Water용매

실험 절차

A solution of 423 mg (1.85 mmol) bis-(4-methoxy-phenyl)-amine in 8 ml acetic acid is treated with 120 mg (1.85 mmol)sodium cyanate. After 4.5 h the reaction mixture is poured onto a solution of 8 g sodium hydroxide in 100 ml water. The resultant precipitate is filtered off and dried.

후처리

  1. filtrationThe resultant precipitate is filtered off
  2. customdried

출처 및 근거

ORD 기록
ord-72bc243ee16e4ae2af60edf972a6d488
출처 데이터셋
uspto-grants-2013_07
특허 번호
US08476286B2

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