Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Fumaric Acid → HCID 86595310, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Fumaric Acid | HCID 444972 | — |
| 반응물 | 2-Chloro-4-(2-(trimethylsilyl)ethynyl)pyridine | HCID 21985391 | — |
| 반응물 | 1-(4-fluoro-phenyl)-4-iodo-2-isopropyl-1H-imidazole | HCID 67304175 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 86595310 | HCID 86595310 | — |
반응 단계
The title compound, MS: m/e=340.1 (M+H+), was prepared in accordance with the general method of example B, step 2, from 2-chloro-4-trimethylsilanylethynyl-pyridine and 1-(4-fluoro-phenyl)-4-iodo-2-isopropyl-1H-imidazole and crystallization from methanol and 1.05 eq fumaric acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08481548B2 |
| 출처 데이터셋 | uspto-grants-2013_07 |
| ORD ID | ord-f5343fcbbb2a489db54c34e4d4af8de5 |
| 출처 메모 | uspto-grants-2013_07 |