Triethylamine → 1246210-02-5
반응식
[F:1][C:2]1([F:11])[CH2:7][CH2:6][CH:5](C(O)=O)[CH2:4][CH2:3]1.C1C=CC(OP([O:24][C:25]2C=CC=CC=2)(N=[N+]=[N-])=O)=CC=1.C([N:33](CC)CC)C>C1(C)C=CC=CC=1>[F:11][C:2]1([F:1])[CH2:3][CH2:4][CH:5]([N:33]=[C:25]=[O:24])[CH2:6][CH2:7]1참가 물질
5
실험 절차
A mixture of 4,4-difluorocyclohexanecarboxylic acid (0.20 g, 1.2 mmol) (Matrix Scientific, Cat. #018320), diphenylphosphonic azide (0.67 g, 2.4 mmol) (Aldrich, Cat. #178756) and triethylamine (0.51 mL, 3.6 mmol) in toluene (10 mL) was refluxed overnight. The volatiles were removed under reduced pressure to afford the product which was directly used for next step reaction without further purification.
후처리
- temperaturewas refluxed overnight
- customThe volatiles were removed under reduced pressure
- customto afford the product which
- customwas directly used for next step reaction without further purification
출처 및 근거
- ORD 기록
- ord-2cc29ac6cfff4aecab4930936f6dced6
- 출처 데이터셋
- uspto-grants-2013_07
- 특허 번호
- US08481732B2
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