Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 2,6-Dichloro-4-iodobenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 2,6-Dichloro-4-iodobenzoic acid | HCID 51341877 | — |
| 생성물 | 2,6-Dichloro-4-iodobenzoyl chloride | HCID 86648958 | 100% |
반응 단계
A solution of 2,6-dichloro-4-iodobenzoic acid (65 mg, 0.21 mmol) in SOCl2 (3 mL) was heated to reflux under nitrogen atmosphere overnight and then cooled to room temperature. The reaction was conentrated under reduced pressure to afford 2,6-dichloro-4-iodobenzoyl chloride (70 mg, 100% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08486950B2 |
| 출처 데이터셋 | uspto-grants-2013_07 |
| ORD ID | ord-4d56422000ae457ca41ed97b75cb9c61 |
| 출처 메모 | uspto-grants-2013_07 |