1H-Pyrazol-3-amine, 5-methyl- → HCID 86649285, 화합물

HRID 450391

반응식

HRID 450391 반응식
[Cl:1][C:2]1[N:7]=[C:6](Cl)[C:5]([N+:9]([O-:11])=[O:10])=[C:4](Cl)[N:3]=1.[CH3:13][C:14]1[NH:18][N:17]=[C:16]([NH2:19])[CH:15]=1.[CH3:20][O-:21].[Na+]>>[Cl:1][C:2]1[N:7]=[C:6]([NH:19][C:16]2[CH:15]=[C:14]([CH3:13])[NH:18][N:17]=2)[C:5]([N+:9]([O-:11])=[O:10])=[C:4]([O:21][CH3:20])[N:3]=1

참가 물질

4

반응물 3

HCID 931461H-Pyrazol-3-amine, 5-methyl-HCID 42978432,4,6-Trichloro-5-nitropyrimidine2회HCID 10942334Sodium Methoxide

생성물 1

HCID 86649285HCID 86649285, 화합물

실험 절차

The title compound was prepared using a procedure similar to the one described for the synthesis of Intermediate 18 using 2,4,6-trichloro-5-nitropyrimidine (Intermediate 37), 5-methyl-1H-pyrazol-3-amine and sodium methoxide as the starting materials. LCMS: 285 [M+1].

출처 및 근거

ORD 기록
ord-142abff36d424c32981f1d185e0f9f1c
출처 데이터셋
uspto-grants-2013_07
특허 번호
US08486966B2

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