Hydroxylamine → 1-[6-(Hydroxymethyl)pyridin-2-yl]ethanone oxime

HRID 450794

반응식

HRID 450794 반응식
[OH:1][CH2:2][C:3]1[N:8]=[C:7]([C:9](=O)[CH3:10])[CH:6]=[CH:5][CH:4]=1.[NH2:12][OH:13]>C(O)C>[OH:1][CH2:2][C:3]1[N:8]=[C:7]([C:9](=[N:12][OH:13])[CH3:10])[CH:6]=[CH:5][CH:4]=1

참가 물질

4

반응물 2

HCID 787HydroxylamineHCID 103294471-(6-(Hydroxymethyl)pyridin-2-yl)ethanone

생성물 1

HCID 1363463671-[6-(Hydroxymethyl)pyridin-2-yl]ethanone oxime

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

To a solution of 1643 mg of 1-[6-(hydroxymethyl)pyridin-2-yl]ethanone in 25 ml of ethanol was added 0.72 ml of a 50% aqueous hydroxylamine solution, followed by stirring overnight. The reaction solution was concentrated under reduced pressure to obtain 1806 mg of 1-[6-(hydroxymethyl)pyridin-2-yl]ethanone oxime as an amorphous substance.

후처리

  1. concentrationThe reaction solution was concentrated under reduced pressure

출처 및 근거

ORD 기록
ord-6ef6da3a33224778a3c3124510f154e5
출처 데이터셋
uspto-grants-2013_07
특허 번호
US08486970B2

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