Hydrochloric Acid → HCID 131730713, 화합물
반응식
[ClH:1].[OH:2][C@@H:3]1[CH2:7][N:6](C(OC(C)(C)C)=O)[C@H:5]([C:15]([O:17][CH2:18][CH:19]=[CH2:20])=[O:16])[CH2:4]1>ClCCl>[ClH:1].[OH:2][C@@H:3]1[CH2:7][NH:6][C@H:5]([C:15]([O:17][CH2:18][CH:19]=[CH2:20])=[O:16])[CH2:4]1참가 물질
4
실험 절차
Hydrochloric acid (4.2 M solution in dioxane, 5 mL, 21 mmol) was added to a solution of 2-allyl 1-tert-butyl (2S,4S)-4-hydroxypyrrolidine-1,2-dicarboxylate (1.05 g, 4.87 mmol) in dichloromethane (20 mL). The resulting mixture was stirred at room temperature for 4 hours then concentrated under vacuum to afford the title compound.
후처리
- concentrationthen concentrated under vacuum
출처 및 근거
- ORD 기록
- ord-e9ef578e304c4b9daa02ee2712567ab5
- 출처 데이터셋
- uspto-grants-2013_07
- 특허 번호
- US08487093B2
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