Methylhydrazine → HCID 59394553, 화합물
반응식
[CH3:1][C:2]1([C:5](=O)[CH2:6][C:7]#[N:8])[CH2:4][CH2:3]1.[CH3:10][NH:11][NH2:12]>CO>[CH3:10][N:11]1[C:7]([NH2:8])=[CH:6][C:5]([C:2]2([CH3:1])[CH2:4][CH2:3]2)=[N:12]1참가 물질
4
실험 절차
A solution of 3-(1-methyl-cyclopropyl)-3-oxo-propionitrile (1.0 g, 8.1 mmol), methylhydrazine (0.56 g, 12.2 mmol) and MeOH (40 mL) is heated at 80° C. for 16 h. The solution is then concentrated in vacuo and the residue is suspended in 5 mL DCM and 20 mL heptane, filtered to give product. MS (ESI) m/z 152.3 (M+1).
후처리
- concentrationThe solution is then concentrated in vacuo
- filtration20 mL heptane, filtered
- customto give product
출처 및 근거
- ORD 기록
- ord-44ffe955ad794a11a8ac015e0bc331ff
- 출처 데이터셋
- uspto-grants-2013_07
- 특허 번호
- US08492393B2
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