Tributyl Phosphate → Lactic Acid

HRID 457250

반응식

HRID 457250 반응식
[C:1]([O-:6])(=[O:5])[CH:2]([CH3:4])[OH:3].[NH4+:7].P(OCCCC)(OCCCC)(OCCCC)=O>>[C:1]([O-:6])(=[O:5])[CH:2]([CH3:4])[OH:3].[NH4+:7].[C:1]([OH:6])(=[O:5])[CH:2]([CH3:4])[OH:3]

참가 물질

4

반응물 2

HCID 31357Tributyl PhosphateHCID 62358Ammonium Lactate

생성물 2

HCID 612Lactic AcidHCID 62358Ammonium Lactate

실험 절차

The procedure described in Example 1 was followed except that 7.57 g of a 70% solution of ammonium lactate was combined with 50 g tributyl phosphate. The reaction mixture was heated for 0.5 hour at 110–118° C. and a reduced pressure of 4.5–5.5 mm Hg, resulting in a conversion of about 97% from ammonium lactate to lactic acid.

후처리

  1. temperatureThe reaction mixture was heated for 0.5 hour at 110–118° C.

출처 및 근거

ORD 기록
ord-f2b98b38f7104dd097424cd92de5d75b
출처 데이터셋
uspto-grants-2007_03
특허 번호
US07186856B2

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