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Dimethyl 2-(4'-methoxy-3-nitrobiphenyl-4-yl)malonate → 4'-Methoxy-3-nitrobiphenyl-4-acetic acid

HRID 457657
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인쇄 미리보기

반응식

HRID 457657 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[CH:14]=[CH:13][C:12]([CH:15](C(OC)=O)[C:16]([O:18]C)=[O:17])=[C:11]([N+:24]([O-:26])=[O:25])[CH:10]=2)=[CH:5][CH:4]=1>Cl>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([C:9]2[CH:14]=[CH:13][C:12]([CH2:15][C:16]([OH:18])=[O:17])=[C:11]([N+:24]([O-:26])=[O:25])[CH:10]=2)=[CH:7][CH:8]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

3

반응물 1

HCID 10737157Dimethyl 2-(4'-methoxy-3-nitrobiphenyl-4-yl)malonate

생성물 1

HCID 104935034'-Methoxy-3-nitrobiphenyl-4-acetic acid

시약·촉매·용매 1

HCID 313Hydrochloric Acid용매

실험 절차

Crude dimethyl 4′-methoxy-3-nitro-biphenyl-4-malonate was heated at 100° C. in 60 mL of 6N hydrochloric acid for 15 hours and cooled. The precipitate was collected by filtration, washed with water and hexane, and dried to give 7.2 g of crude 4′-methoxy-3-nitrobiphenyl-4-acetic acid as a light tan solid.

후처리

  1. temperaturecooled
  2. filtrationThe precipitate was collected by filtration
  3. washwashed with water and hexane
  4. customdried

출처 및 근거

ORD 기록
ord-8fe8e55af71a4b3a9b307dfed7e92006
출처 데이터셋
uspto-grants-2007_03
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07189721B2

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