Salicylaldehyde → HCID 69497707, 화합물

HRID 460662

반응식

HRID 460662 반응식
[CH:1](=O)[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[C:10]1(=[O:16])[O:15][CH:13]([CH3:14])[CH2:12][CH2:11]1>C1(C)C=CC=CC=1>[OH:4][C:3]1[CH:5]=[CH:6][CH:7]=[CH:8][C:2]=1[CH:1]=[C:11]1[CH2:12][CH:13]([CH3:14])[O:15][C:10]1=[O:16]

참가 물질

4

반응물 2

HCID 6998SalicylaldehydeHCID 7921Gamma-Valerolactone

생성물 1

HCID 69497707HCID 69497707, 화합물수율 66.9%

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

Salicylaldehyde (15.2 g) and γ-valerolactone (25 g) were dissolved in toluene (150 ml). By the reactions as in the same manner as in Example 307, the title compound (17 g) was obtained, melting point 112–114° C.

출처 및 근거

ORD 기록
ord-b7558b236a9d4731b3ff9f454b289deb
출처 데이터셋
uspto-grants-2007_03
특허 번호
US07196199B2

연결된 노트

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