N,N'-Diethylthiourea → 3-Ethyl-2-ethylimino-4-(2,4-dichloro-5-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrobromide

HRID 460820

반응식

HRID 460820 반응식
[Br:1][CH2:2][C:3]([C:5]1[CH:10]=[C:9]([S:11](=[O:14])(=[O:13])[NH2:12])[C:8]([Cl:15])=[CH:7][C:6]=1[Cl:16])=[O:4].[CH2:17]([NH:19][C:20]([NH:22][CH2:23][CH3:24])=[S:21])[CH3:18]>>[BrH:1].[CH2:23]([N:22]1[C:3]([C:5]2[CH:10]=[C:9]([S:11](=[O:14])(=[O:13])[NH2:12])[C:8]([Cl:15])=[CH:7][C:6]=2[Cl:16])([OH:4])[CH2:2][S:21][C:20]1=[N:19][CH2:17][CH3:18])[CH3:24]

참가 물질

3

반응물 2

HCID 2735009N,N'-DiethylthioureaHCID 227564292-Bromo-2',4'-dichloro-5'-sulfamoylacetophenone

생성물 1

HCID 213947703-Ethyl-2-ethylimino-4-(2,4-dichloro-5-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrobromide

실험 절차

was obtained in a manner analogous to that described in Example 1 d) from 3.5 g of 2-bromo-2',4'-dichloro-5'-sulfamoyl-acetophenone and 1.3 g of 1,3-diethyl-thiourea. M.p. 202° C (decomposition).

후처리

  1. customwas obtained in a manner analogous to
  2. customthat described in Example 1 d

출처 및 근거

ORD 기록
ord-0cddd439074d4f16a1cd7714e865d04f
출처 데이터셋
uspto-grants-1977_12
특허 번호
US04061647

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